Discovery of 63286-28-2

According to the analysis of related databases, 63286-28-2, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 63286-28-2, name is 2-Chloro-3-hydrazinylpyrazine, This compound has unique chemical properties. The synthetic route is as follows., Product Details of 63286-28-2

Intermediate B-1 (15.6 g; 108 mmol) is slurried up in THF (300 ml_) and cooled down in an ice bath to – 5 C. Trifluoroacetic anhydride (17 ml118 mmol) is also dissolved in 300 ml_ THF and dropped slowly to the first solution. After 1 h most of the THF is evaporated, then a small amount of water is added and the mixture is extracted with DCM. The organic phase is dried over MgS04 and evaporated to dryness. (0283) Yield: 100 % HPLC-MS: (M+H)+ = 241/243; tRet = 1.31 min; method FSUN2

According to the analysis of related databases, 63286-28-2, the application of this compound in the production field has become more and more popular.

Reference:
Patent; BOEHRINGER INGELHEIM INTERNATIONAL GMBH; TONTSCH-GRUNT, Ulrike; BAUM, Anke; RUDOLPH, Dorothea Ingrid; (85 pag.)WO2019/145410; (2019); A1;,
Pyrazine – Wikipedia,
Pyrazine | C4H4N2 – PubChem