Discovery of 109-08-0

The synthetic route of 109-08-0 has been constantly updated, and we look forward to future research findings.

In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 109-08-0, name is 2-Methylpyrazine belongs to pyrazines compound, it is a common compound, a new synthetic route is introduced below. Product Details of 109-08-0

General procedure: The preparation of co-crystals 1e3 was conducted through solutioncrystallization experiments. Co-crystal 1 was obtained usingthe following procedure: MP (0.25 mmol, 23.5 mg) and 4-HIPA(0.5 mmol, 91.1 mg), in a 1:2 stoichiometric ratio, were dissolvedin separate beakers in 15 mL of methanol, and subsequently combinedtogether. The resulting solutionwas left to evaporate at roomtemperature. Two weeks later, colorless block-like co-crystals of 1were obtained. (yield87percent, based on 2-methylpyrazine). Elementalanalysis for co-crystal 1, Anal. Calcd. (percent): C, 55.03; H, 3.96; N, 6.11.Found: C, 54.96; H, 3.98; N, 6.17. IR (KBr pellet, cm1): 3435, 2918,2517,1682,1588,1441,1400,1360,1281,1244,1225,1174,1067,1040,934, 806, 775, 690, 633, 566, 519.

The synthetic route of 109-08-0 has been constantly updated, and we look forward to future research findings.

Reference:
Article; Wen, Gao-Ju; Gu, Lian-Shuai; Sun, Bai-Wang; Journal of Molecular Structure; vol. 1150; (2017); p. 96 – 102;,
Pyrazine – Wikipedia,
Pyrazine | C4H4N2 – PubChem