Related Products of 5910-89-4, A common heterocyclic compound, 5910-89-4, name is 2,3-Dimethylpyrazine, molecular formula is C6H8N2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
2.56 g of 2,3-dimethyl-pyrazine (23.67 mmol) was dissolved in 100 mL of ethanol with 2.1 g 10% palladium on active carbon. The reaction mixture was hydrogenated under pressure (55-60 psi) for 3 days. The solid was filtered and removed. The filtrate was concentrated to afford 3.0 g of 2,3-dimethylpiperazine, which was used without purification. 1H NMR (400 MHz, CDCl3), delta (ppm): 2.95 (m, 4H), 2.74 (m, 2H), 1.04 (d, 6H).
The synthetic route of 5910-89-4 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Kalypsys, Inc.; US2005/234046; (2005); A1;,
Pyrazine – Wikipedia,
Pyrazine | C4H4N2 – PubChem