Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 123-32-0, name is 2,5-Dimethylpyrazine, A new synthetic method of this compound is introduced below., Safety of 2,5-Dimethylpyrazine
General procedure: A mixture of AgNO3 (0.051 g, 0.3 mmoL), H2ntph (0.063 g, 0.3mmol) and pyz (0.024 g, 0.3 mmoL) were dissolved in H2O/acetonitrile(10 mL, 1:1), after stirred for 20 min in air and then the mixturewas transferred to a 25 mL stainless steel reactor and heatedto 110 C for 72 h. And then the reaction system was cooled toroom temperature, colorless needle crystals of 1 were obtained.Yield based on Ag: 72%.
The synthetic route of 123-32-0 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Yang, Yuan-Yuan; Zhou, Lin-Xia; Zhu, Hong-Lin; Li, Wen-Ying; Zheng, Yue-Qing; Polyhedron; vol. 148; (2018); p. 161 – 170;,
Pyrazine – Wikipedia,
Pyrazine | C4H4N2 – PubChem