Related Products of 14667-55-1, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 14667-55-1 as follows.
General procedure: AgNO3 (34.2 mg, 0.2 mmol), tpyz (38 ml, 0.2 mmol) and H2L(313.6 mg, 0.2 mmol) were took place in CH3CN-DMF (N,Ndimethylformamide)mixed solvent (6 ml, v/v: 3/3) under stirring.Then, ammonia (14 M, 10 d) was dropped into the mixture to give aclear solution under ultrasonic treatment (160 W, 40 KHz, 30 min) atroom temperature. The resultant solution was allowed to evaporateslowly in darkness at room temperature for several days to giveirregular-yellow crystals of 1 (Yield: 32%, based on Ag).
According to the analysis of related databases, 14667-55-1, the application of this compound in the production field has become more and more popular.
Reference:
Article; Huang, Hua-Qi; Cheng, Xiao-Yue; Zhang, Ting; Huang, Rong-Bin; Inorganic Chemistry Communications; vol. 68; (2016); p. 21 – 28;,
Pyrazine – Wikipedia,
Pyrazine | C4H4N2 – PubChem